Organic Chemistry lab

Eight 20.0 mmol of isopentyl alcohol into a 10 ml round bottom flask match magnetic stir seal off Add 2.3 ml of glacial acetic acid past stir the mixutre Add .15 ml of concentrated sulfuric acid Connect a peeing cooled condenser to the chemical reception flask figure out on the alter weewee and heat Reduce the heating rate if the reflux family rises to in spite of appearance 2cm of the top of the condenser When the reaction time is up render the reaction mixture to cool to nearly room temperature. exercise off the cooling water and remove the condenser with a few drops of water Transfer the reaction mixture to a love cap extractor tube and add 6 ml of aft(prenominal) using some of the after for the graft Ash the reaction mix with the after and remove cautiously Pressure may build up in the caped centrifuge tube During the first washables stir the layers until gas growth subsides before you cap the centrifuge tube and vent it a great deal Try to remove all of the sedimentary layer after the last washing to minimize the hail of water in the product Dry the crude isopentyl acetate by adding a small amount of anhydrous sodium sulfate conservatively transfer the limpid to a dry 5ml conical ampoule using a dry filter tip pipet Try not to transfer any drying agent with the liquid M.W b.p d solubility Acetic acid 60.

1 118 1.049 miscible Isopentyl alcohol 88.1 130 0.815 2.7 Isopentyl acetate 130.2 142 0.876 0.25 sulphuric ! acid 98.1 290 1.84 miscibleIf you indirect request to get a full essay, revise it on our website: OrderEssay.net

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